Polyhedron – Electrometric
Analytical Methods
Polyhedron Laboratories utilizes electrometric
analytical methods performed to ASTM standards, such as Acidity or
Alkalinity by Potentiometric Titration (ASTM D2896-06), Chloride
(ASTM F1277-02), Conductivity (ASTM D1125-95), and pH Measurement
(ASTM E70-97). All ASTM standard descriptions below are paraphrased
from the ASTM website (www.astem.org). Due to copyright restrictions, Polyhedron
Laboratories cannot make available copies of standards.
Standards can be found and are available at www.astm.org.
ASTM D2896-06
Standard Test Method
for Base Number of Petroleum Products by Potentiometric Perchloric
Acid Titration - This test procedure deals with the determination of
basic specimens in products by titration with perchloric acid in
glacial acetic acid. Test procedures A and B use different titration
solvent volumes and sample weights. Additionally, this test method
allows for the use of an alternative solvent structure, which
eliminates the use of chlorobenzene. The constituents considered to
have basic characteristics include amino compounds, organic and
inorganic bases, basic salts of polyacidic bases, salts of weak
acids (such as soaps), and salts of heavy metals.
ASTM F1277-02
Standard Test Method
for Determination of Leachable Chloride in Materials by
Ion-Selective Electrode Technique - This test procedure allows for
the measurement of chloride ion leached from plastics and
composites. Samples containing 7 to 6700 g Cl-/g sample can be
analyzed using this method. The upper concentration threshold is
extendable by the dilution of the test solution.
ASTM D1125-95
Standard Test Methods for Electrical Conductivity and Resistivity of Water - The
following test procedures deal with the determination of the
electrical conductivity and resistivity of water. The test methods
are as follows – Test Method A - Field and Routine Laboratory
Measurement of Non-Flowing (Static) Specimens (Range from 10 to
200,000 S/cm, Sections 12 to 18); Test Method B – Continuous
In-Line Measurement (Range from 5 to 200,000 S/cm, Sections 19 to
23). The test procedures have been tested in reagent water.
ASTM E70-97 Standard Test Method for
pH of Aqueous Solutions With the Glass Electrode - This test
procedure defines the equipment and methods for the electrometric
measurement of pH values of aqueous solutions with the glass
electrode.
| Acidity or Alkalinity by
Potentiometric Titration |
ASTM D 2896 |
| Chloride |
ASTM F 1277 |
| Conductivity |
ASTM D 1125 |
| Hydroperoxide by Dead
Stop Iodometric Titration |
|
| pH Measurement |
ASTM E 70 |
|